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Synchrotron X ray absorption student projects in community college and gateway for chemical engineering related education

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Conference

2024 ASEE North East Section

Location

Fairfield, Connecticut

Publication Date

April 19, 2024

Start Date

April 19, 2024

End Date

April 20, 2024

Page Count

9

DOI

10.18260/1-2--45750

Permanent URL

https://peer.asee.org/45750

Download Count

23

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Paper Authors

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Sunil Dehipawala City University of New York, Queensborough Community College

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Sunil Dehipawala received his B.S. degree from University of Peradeniya in Sri Lanka and Ph.D from City University of New York. Currently, he is working as a faculty member at Queensborough Community College of CUNY and engages in material research.

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Lexi grace Robinson

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Harsha Rajapakse

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A committed chemist, researcher, educator, and innovator with an unwavering desire for excellence, clarity of reflection, multi-disciplinary learning accomplishments, ground-breaking innovations, collaborative studies, entrepreneurship, intellectual and ethical responsibility, and service to the scientific, national, and international communities.

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Tak Cheung

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Tak Cheung, Ph.D., professor of physics, teaches in CUNY Queensborough Community College. He also conducts research and mentors student research projects.

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Abstract

A Synchrotron radiation student project in our community college consists of data collection, data analysis, and discussion which includes the formulation of a new hypothesis. Although the on-site data collection at National Labs such as NSLS II at BNL, Cornell High Energy Synchrotron Source are limited by the Synchrotron beam time availability students were able to participate on site data analysis from previously collected data. The data analysis component fully engages the students in Extended X ray Absorption Fine Structure(EXAFS), X ray absorption Near Edge Structure (XANES), and X ray absorption pre edge feature analysis. These tools were used to analyze microstructure of iron and zinc compounds in a variety of samples. In EXAFS experiments data consists of absorption coefficient of element under investigation versus X ray energy at the vicinity of an absorption edge and about 200 eV below & 1000 eV above the edge energy. Analysis of EXFS data yields the amount of the element under investigation and structural parameters such as oxidation state, near neighbor bond length, number of near neighbor atoms and disorder. The advantage of this method is minimal sample preparation and no chemical treatments to samples. The pedagogy encourages mindful reading of the latest Synchrotron based research articles with faculty guidance to build a relationship to a chemical engineering related education. The pedagogy of using the Synchrotron radiation student projects in community college has been found to broaden the prospect and build connections to chemical engineering related education in the senior college setting. The data analysis steps of several different material and structure interpretations will be presented.

Dehipawala, S., & Robinson, L. G., & Rajapakse, H., & Cheung, T. (2024, April), Synchrotron X ray absorption student projects in community college and gateway for chemical engineering related education Paper presented at 2024 ASEE North East Section, Fairfield, Connecticut. 10.18260/1-2--45750

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